Transformation of potentially toxic lead to crystalline Pb (NO3)2

Authors

  • Ulises Alejandro Villalón López Faculty of Chemical Sciences and Engineering, UABC. Calzada Universidad, 14418, Industrial Park Tijuana International, 22390, Tijuana, Baja California, Mexico. https://orcid.org/0000-0002-7429-8546
  • María Guadalupe Moreno Armenta Center for Nanosciences and Nanotechnology, UNAM. Km. 107 Carretera Tijuana-Ensenada, CP 22800, Ensenada, Baja California, Mexico. https://orcid.org/0000-0002-8040-0615
  • Arturo Barrera Rodríguez University of Guadalajara, University Center of the Ciénega, Av. Universidad, Number 1115, Col. Linda Vista, Apdo. Postal 106, Ocotlán Jalisco, Mexico. https://orcid.org/0000-0003-2788-7425
  • Eduardo Rogel Hernández Faculty of Chemical Sciences and Engineering, UABC. Calzada Universidad, 14418, Industrial Park Tijuana International, 22390, Tijuana, Baja California, Mexico. https://orcid.org/0000-0003-2746-8116
  • Juan Manuel Quintana Melgoza Faculty of Chemical Sciences and Engineering, UABC. Calzada Universidad, 14418, Industrial Park Tijuana International, 22390, Tijuana, Baja California, Mexico. https://orcid.org/0000-0002-3738-0612

DOI:

https://doi.org/10.37636/recit.v23106112

Keywords:

Toxic residual lead, Chemical synthesis, Lead nitrate product.

Abstract

The accumulation of lead in the environment is a cause of health problems in humans. The mean lethal dose reported in mg/kg for Pb, Pb(NO3)2 and PbO is 400, 2250 and 2000, respectively. Due to the high toxicity of metallic lead with respect to lead nitrate, a methodology has been developed to transform residual lead into lead nitrate, whose toxicity is five times lower than metallic lead. On the other hand, lead nitrate can be a precursor for the synthesis of materials with potential industrial application. The synthesis of Pb(NO3)2 is carried out by mixing the residual metallic lead and 15.7 molar nitric acid in a proportion of reagents [1:4]. Subsequently, the mixture is subjected to magnetic stirring to dissolve the lead and form a white precipitate, dried at 110 ° C for 1 h obtaining an experimental yield of 99 %. The synthesized material is characterized by X–ray diffraction, scanning electron microscopy and energy dispersion spectroscopy. Likewise, this methodology has a favorable impact on ecosystems, since lead contamination will be diminished.

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SEM micrograph of Pb (NO3) 2 synthesized from metallic lead.

Published

2019-09-25

How to Cite

Villalón López, U. A., Moreno Armenta, M. G., Barrera Rodríguez, A., Rogel Hernández, E., & Quintana Melgoza, J. M. (2019). Transformation of potentially toxic lead to crystalline Pb (NO3)2. Revista De Ciencias Tecnológicas, 2(3), 106–112. https://doi.org/10.37636/recit.v23106112

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